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PRODUCTION OF HIGHLY GRAPHITIZED MULTIWALlED CARBON ANOTUBES

X.L.Zhao1) , T.L.Guo2) , M.Ohkohchi3) , T.Okazaki3) , S.Iijima and Y.Ando3) 1) Japan Science and Technology Corporation , Department of Physics , Meijo University , Shiogamaguchi1 501 , Tempaku ku , Nagoya 468 8502 , Japan 2) Scientific Research Department , Shenyang University , Wanghuanan Street21 , Dadong District , Shenyang 110044 , China 3) Department of Physics , Meijo University , Shiogamaguchi 1 501 , Tempaku ku , Nagoya 468 8502 , Japan$

金属学报(英文版)

Multiwalled carbon nanotubes ( MWNTs) were prepared by DCarc dischargein hydrogen gas, and werethermally purified byinfrared radiation in air. The morphology of pristineand purified MWNTs was observed by scanning electron microscope ( SEM) , and the crys tallinestructureand perfection wereinvestigated by high resolution transmission electron mi croscope( HRTEM) and Raman spectrometer. Itcameto the conclusion thatthese MWNTs possessed a high degreeof graphitization and very narrow centralchannel(about1 0 nm indiameter) , giving risetotheappearanceof breathing modesfor MWNTs.

关键词: multiwalled carbon nanotubes , null , null , null , null

STRUCTURE AND MAGNETIC PROPERTIES OF Fe/Pd COMPOSITIONALLY MODULATED FILMS

ZHANG Lin , LIU Yihua Shandong University , Jinan , China WANG Hao Dongnan University , Nanjing , China engineer , Department of Physics , Shandong University , Jinan 250100 , China

金属学报(英文版)

Metal Fe/Pd compositionally modulated films(CMFs) were prepared by vapour depo- sition from two sources onto glass substrate under vacuum.The modulation and crystal structures of the films were examined by X-ray diffraction.The magnetic properties were determined by vibrating sample magnetometer.The Pd layers in the Fe/Pd CMFs are of fcc structure,and the Fe layer structure transits from bcc into amorphous,state with decreasing thickness of Fe layer.The dependence of specific saturation magnetization on thickness of Fe layers has also been discussed.

关键词: compositionally modulated films , null , null

DESIGN CONCEPT FOR SNAP-ACTING TWO-WAY SHAPE MEMORY DEVICES

LIN Guangming CHENXingyuan ZHANG Jinxiu Material Science Research Institute , Zhongshan University , Guangzhou , China WANG Yurui Metallurgy Research Institute of Beijing Iron and Steel Company , Beijing , China LIN Guangming Associate Professor , Department of Physics , Zhongshan University , Guangzhou 510275 , China

金属学报(英文版)

Snap-acting two way shape memory device can be obtained by using the design proposed by authors.Some essential parameters which characterize the properties of device have been pro- posed also in this paper.And the principle and method according to which a practical snap-acting device can be designed have been described.

关键词: shape memory alloy , null , null

IN SITU TEM OBSERVATION OF MICROSTRUCTURES OF AUSTENITIC-0.45%C STEELS WELD JOINT

PAN Chunxu SHI Yuxiang WANG Renhui GUI Jianian Wuhan University , Wuhan , China Wuhan University of Water Transportation Engineering , Wuhan , China Professor , Department of Physics , Wuhan University , Wuhan , China

金属学报(英文版)

The successive alteration o the microstructure from the weld metal zone through weld bond to the heat affected zone of a Cr18Ni13 austenitic-0.45%C steels weld joint was observed in situ using transmission electron microscopy.It was found a new type of microstructure called pearlite-like structure and observed the characteristics of the boundary of dissimilar phases. Based on the definition of various zones of the dissimilar steels weld joint under the optical mi- croscope,the transmission electron microscopic characteristics,including microstructures and compositions,of each zone are described and discussed.

关键词: weld joint microstructure , null , null

稀土对工业纯铁中温内耗的影响

戢景文 , 赖祖涵 , 吴玉琴 , 张国福 , 李广义

金属学报

研究了稀土对工业纯铁中温内耗的影响.结果表明:其影响程度和热处理过程密切相关,铁中稀土有合金化作用.炉冷后变形铁在600℃时效,仍存在Snoek Ke-Koster(以下简称SKK)峰;随时效温度升高,SKK峰温度T_p不是单一下降,在600℃时效出现明显回升。

关键词: 内耗 , associate professor , Department of Physics

CORRELATION BETWEEN STRESS COMPONENTS AND STRESS CORROSION CRACKS IN BRASS Lecturer,Department of Materials Physics,University of Science and Technology Beijing,Beijing 100083,China

QIAO Lijie LIU Rui XIAO Jimei University of Science and Technology Beijing , Beijing , China

金属学报(英文版)

The effects of stress components on nucleation sites and propagation directions of stress cor- rosion cracks in brass were investigated with specimens under mode Ⅱ and mode Ⅲ loadings. The results indicated that under mode Ⅱ loading,stress corrosion cracks nucleated on the site with maximum normal stress component and propagated along the plane perpendieular to the maximum normal stress,under mode Ⅲ loading,the stress corrosion crack was not evident on the 45°plane due to the general corrosion in aqueous solution with high NH_4OH concentra- tion,while stress corroded in aqueous solution with low NH_4OH concentration, numerous cracks with spacings of 10—150μm were found on the 45°plane with maximum normal stress and no stress corrosion cracks was observed on the plane with maximum shear stress.

关键词: stress corrosion cracking , null , null , null

CURRENT STATUS OF HIGH-RESOLUTION ELECTRON-MICROSCOPY AND ITS APPLICATIONS TO MATERIALS SCIENCE AND CONDENSED MATTER PHYSICS

材料科学技术(英)

The present paper summarizes the current status of high resolution elect;on microscopy ( HREM) and the applications of HREM to materials science and condensed matter physics. This review recounts the latest development of high resolution electron microscope, progress of HREM and the applications of HREM, including the crystal structure determination of microcrystalline materials and characterization of the local structure of the defects and nanostructured materials as well as qualitative and quantitative analysis of the grain boundaries, interfaces and interfacial reactions in the advanced materials by means of HREM in combination with electron diffraction, subnanometer level analysis, image simulation and image processing.

关键词: juxtaposed pentagonal antiprisms;two-dimensional quasicrystal;domain;boundary structures;close-packed phases;nanocrystalline materials;crystal-structure;copper oxidation;initial-stage;translational;symmetry;rotational symmetry

Current Status of High Resolution Electron Microscopy and Its Applications to Materials Science and Condensed Matter Physics

Douxing LI and Hengqiang YE (Laboratory of Atomic imaging of Solids , Institute of Metal Research , Chinese Academy of Sciences , Shenyang , 110015 , China)

材料科学技术(英)

The present paper summarizes the current status of high resolution electron microscopy (HREM)and the applications of HREM to materials science and condensed matter physics. This review recounts the latest development of high resolution electron microscope, progress of HREM and the applications of HREM, including the crystal structure determination of microcrystalline materials and characterization of the local structure of the defects and nanostructured materials as well as qualitative and quantitative analysis of the grain boundaries, interfaces and interfacial reactions in the advanced materials by means of HREM in combination with electron diffraction,subnanometer level analysis, image simulation and image processing.

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